A Novel Method of Combining Solid Phase Extraction with Solidified Floating Organic Drop Microextraction for Speciation of Inorganic Arsenic in Wastewater Samples by Electrothermal Vaporization ICP-MS
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چکیده
منابع مشابه
Determination of Cadmium by Electrothermal Atomic Absorption Spectrometry after its Separation and Preconcentration by Syringe to Syringe Dispersive Liquid Phase Microextraction-Solidified Floating Organic Drop
The application of syringe to syringe dispersive liquid phase microextraction-solidified floating organic drop was extended for the separation and preconcentration of trace amounts of cadmium ions from water and cereal samples. The extracted cadmium was quantified by electrothermal atomic absorption spectrometry. Factors affecting the complex formation as well as microextraction efficiency such...
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A novel method was developed for determination of trace amounts of lead in water and food samples. Solidified floating organic drop microextraction was used to preconcentrate the lead ion. After the analyte was complexed with 1-(2-pyridylazo)-2-naphthol, undecanol and acetonitrile were added as extraction and dispersive solvent, respectively. Variables such as pH, volumes of extraction and disp...
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Electrothermal vaporization with two filaments was studied for low-pressure helium-ICP-MS. A 10-microl volume of sample was dried and vaporized, and then introduced to the ICP. With this technique, four elements were simultaneously determined with the acceptable precisions (RSD ca. 10%). The detection limit based on 3sigma of background signals approached the fractional ppb range. The proposed ...
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ژورنال
عنوان ژورنال: Atomic Spectroscopy
سال: 2017
ISSN: 0195-5373,2708-521X
DOI: 10.46770/as.2017.01.003